Diethyl pyridin-3-ylphosphonate → HCID 23117755, 화합물

HRID 1360660노트

반응식

HRID 1360660 반응식
[N:1]1[CH:6]=[CH:5][CH:4]=[C:3]([P:7](=[O:14])([O:11][CH2:12][CH3:13])[O:8][CH2:9][CH3:10])[CH:2]=1.[H][H]>CCO.C(O)(=O)C.[Pt]=O>[NH:1]1[CH2:6][CH2:5][CH2:4][CH:3]([P:7](=[O:14])([O:11][CH2:12][CH3:13])[O:8][CH2:9][CH3:10])[CH2:2]1

참가 물질

5

반응물 2

HCID 10867660Diethyl pyridin-3-ylphosphonateHCID 178418361HCID 178418361, 화합물

생성물 1

HCID 23117755HCID 23117755, 화합물

시약·촉매·용매 2

HCID 82844Platinum oxide (PtO)용매HCID 18476134Acetic acid ethanol용매

실험 절차

Diethyl pyridin-3-ylphosphonate was dissolved in EtOH-acetic acid, to which platinum oxide was added, for stirring under 3.4 kgf/cm2 hydrogen for 120 hours, to obtain diethyl piperidin-3-ylphosphonate.

후처리

  1. additionwas added

출처 및 근거

ORD 기록
ord-6f29a44ea6344498b3ae599f3eda33a1
출처 데이터셋
uspto-grants-2011_02
특허 번호
US07879878B2

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