Trifluoroacetic acid → HCID 66727110, 화합물
반응식
C(OC(=O)[NH:7][CH2:8][C:9]1[CH:14]=[CH:13][N:12]=[C:11]2[NH:15][CH:16]=[CH:17][C:10]=12)(C)(C)C.[F:19][C:20]([F:25])([F:24])[C:21]([OH:23])=[O:22]>C(Cl)Cl>[F:19][C:20]([F:25])([F:24])[C:21]([OH:23])=[O:22].[NH:15]1[C:11]2=[N:12][CH:13]=[CH:14][C:9]([CH2:8][NH2:7])=[C:10]2[CH:17]=[CH:16]1참가 물질
4
실험 절차
To a solution of (1H-pyrrolo[2,3-b]pyridin-4-ylmethyl)-carbamic acid tert-butyl ester (200 mg, 0.809 mmol) in CH2Cl2 (6 mL) was added trifluoroacetic acid (1.58 mL, 20.6 mmol). After 14 hours, the reaction was concentrated in vacuo to afford the title compound which was used in the without purification.
후처리
- concentrationthe reaction was concentrated in vacuo
출처 및 근거
- ORD 기록
- ord-bb0f72b1bdfc4c69a5e02dd815fadc51
- 출처 데이터셋
- uspto-grants-2011_02
- 특허 번호
- US07879873B2
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