Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-Naphthoyl chloride → 3-{4-[(Naphthalene-2-carbonyl)-amino]-phenyl)-acrylic acid methyl ester
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-Naphthoyl chloride | HCID 75246 | — |
| 반응물 | 2-Propenoic acid, 3-(4-aminophenyl)-, methyl ester | HCID 3017578 | — |
| 생성물 | 3-{4-[(Naphthalene-2-carbonyl)-amino]-phenyl)-acrylic acid methyl ester | HCID 66958345 | — |
반응 단계
Using an analogous method (H4), the title compound was prepared from 2-naphthalenecarbonyl chloride (0.557 g, 2.91 mmol) and 3-(4-amino-phenyl)-acrylic acid methyl ester (3) in a form of white solid (0.950 g, 75%). 1H NMR (DMSO-d6, HMDSO), δ: 3.65 (3H, s); 6.51 (1H, d, J=16.0 Hz); 7.47-8.25 (12H, m); 10.63 (1H, s).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07880020B2 |
| 출처 데이터셋 | uspto-grants-2011_02 |
| ORD ID | ord-94d7b429993b4eb68202734b1cc6d13d |
| 출처 메모 | uspto-grants-2011_02 |