Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Isopropylamine → 2-Amino-N-isopropylbenzamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Isopropylamine | HCID 6363 | — |
| 반응물 | Isatoic Anhydride | HCID 8359 | — |
| 용매 | Water | HCID 962 | — |
| 생성물 | 2-Amino-N-isopropylbenzamide | HCID 94411 | 77.1% |
반응 단계
A round-bottomed flask was charged with isatoic anhydride (5.0 g, 0.030 mol) and 30 mL water. Isopropylamine (4.64 mL, 0.049 mol) was added slowly to the reaction mixture. The product precipitated from the reaction mixture. After 1 h, the reaction mixture was filtered and washed with water to give 4.12 g (71% yield) of a white solid
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07884098B2 |
| 출처 데이터셋 | uspto-grants-2011_02 |
| ORD ID | ord-7fc24b27a8664e549d66df96405fa8cf |
| 출처 메모 | uspto-grants-2011_02 |