Pyridinium chloride → HCID 66933697, 화합물

HRID 1363358노트

반응식

HRID 1363358 반응식
[Cl:1][C:2]1[CH:3]=[C:4]([C:8]2[O:9][C:10]3[C:15]([C:16](=[O:18])[CH:17]=2)=[C:14]([O:19]C)[CH:13]=[C:12]([O:21]C)[C:11]=3[C@@H:23]2[CH2:27][CH2:26][N:25]([CH3:28])[C@H:24]2[CH2:29][OH:30])[CH:5]=[CH:6][CH:7]=1.Cl.N1C=CC=CC=1>>[Cl:1][C:2]1[CH:3]=[C:4]([C:8]2[O:9][C:10]3[C:15]([C:16](=[O:18])[CH:17]=2)=[C:14]([OH:19])[CH:13]=[C:12]([OH:21])[C:11]=3[C@@H:23]2[CH2:27][CH2:26][N:25]([CH3:28])[C@H:24]2[CH2:29][OH:30])[CH:5]=[CH:6][CH:7]=1

참가 물질

3

반응물 2

HCID 10176127Pyridinium chlorideHCID 66933637HCID 66933637, 화합물

생성물 1

HCID 66933697HCID 66933697, 화합물

실험 절차

Compound of example 73 (0.25 g, 0.58 mmol) was subjected to demethylation using pyridine hydrochloride (2.5 g, 21.64 mmol) as described in example 17 to afford the title compounds.

출처 및 근거

ORD 기록
ord-7ffda5bb880649bca9a018ebb8c8fd93
출처 데이터셋
uspto-grants-2011_02
특허 번호
US07884127B2

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