Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Water → 2,2-diethoxyethyl Benzoate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Water | HCID 962 | — |
| 반응물 | Dimethylformamide | HCID 6228 | — |
| 반응물 | 2-Chloro-1,1-diethoxyethane | HCID 12128 | — |
| 반응물 | Potassium Benzoate | HCID 23661960 | — |
| 용매 | Ethyl Acetate | HCID 8857 | — |
| 생성물 | 2,2-diethoxyethyl Benzoate | HCID 11817258 | 30% |
반응 단계
Chloroacetaldehyde diethyl acetal (1.9 g), potassium benzoate (2.0 g) and DMF (20 mL) were placed in a three-neck flask, followed by refluxing. Twenty hours later, the reaction mixture was cooled to room temperature, and water (60 mL) and ethyl acetate (80 mL) were added thereto, followed by stirring. After filtration and separation, the organic layer was concentrated and thereby yielded the target compound (0.69 g) in a yield of 30%.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07728152B2 |
| 출처 데이터셋 | uspto-grants-2010_06 |
| ORD ID | ord-ab04dd03fbe84d7fa44f135c7f0202f5 |
| 출처 메모 | uspto-grants-2010_06 |