Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Potassium Iodide → methyl (4E)-2-acetyl-5-phenyl-4-pentenoate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Potassium Iodide | HCID 4875 | — |
| 반응물 | Cinnamyl bromide | HCID 5357478 | — |
| 반응물 | sodium (2E)-4-methoxy4-oxo-2-buten-2-olate | HCID 23681258 | — |
| 생성물 | methyl (4E)-2-acetyl-5-phenyl-4-pentenoate | HCID 11020753 | — |
반응 단계
Analogously to Example 28A, 10 g (72.4 mmol) of sodium (2E)-4-methoxy-4-oxo-2-buten-2-olate and 0.40 g (2.41 mmol) of potassium iodide are reacted with 14.3 g (72.4 mmol) of [(1E)-3-bromo-1-propenyl]benzene to give methyl (4E)-2-acetyl-5-phenyl-4-pentenoate.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06573263B2 |
| 출처 데이터셋 | uspto-grants-2003_06 |
| ORD ID | ord-bbee9c6118c04db7923aaaa574d1a179 |
| 출처 메모 | uspto-grants-2003_06 |