Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 1368523생성일: 2026년 10월 26일
1-(6-Acetoxynaphthalen-2-yl)-1-(1-trityl-1H-imidazol-4-yl)-2-methyl-1-propanol → HCID 178475354, 화합물
https://huagongshe.com/reaction/1368523
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | 1-(6-Acetoxynaphthalen-2-yl)-1-(1-trityl-1H-imidazol-4-yl)-2-methyl-1-propanol | HCID 22018342 | — |
| 촉매 | HCID 178418390 | HCID 178418390 | — |
| 용매 | Acetic Acid | HCID 176 | — |
| 생성물 | HCID 178475354 | HCID 178475354 | 69.9% |
반응 단계
1-(6-Acetoxynaphthalen-2-yl)-1-(1-trityl-1H-imidazol-4-yl)-2-methyl-1-propanol (0.25 g) was dissolved in acetic acid (20 ml). To the mixture was added 10% palladium carbon (0.1 g). The mixture was stirred at 50° C. for 2 h under hydrogen atmosphere. The catalyst was filtered off, and filtrate was concentrated. The residue was purified by silica gel chromatography (eluent; dichloromethane-methanol=10:1) to give the titled compound (0.1 g) as a colorless solid.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| 특허 번호 | US06573289B1 |
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| 출처 데이터셋 | uspto-grants-2003_06 |
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| ORD ID | ord-294df26305144dcbba769b9e9633acc5 |
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| 출처 메모 | uspto-grants-2003_06 |
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