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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 1368523생성일: 2026년 10월 26일

1-(6-Acetoxynaphthalen-2-yl)-1-(1-trityl-1H-imidazol-4-yl)-2-methyl-1-propanol → HCID 178475354, 화합물

https://huagongshe.com/reaction/1368523

반응식

참여 물질

역할이름HCID투입량
반응물1-(6-Acetoxynaphthalen-2-yl)-1-(1-trityl-1H-imidazol-4-yl)-2-methyl-1-propanolHCID 22018342—
촉매HCID 178418390HCID 178418390—
용매Acetic AcidHCID 176—
생성물HCID 178475354HCID 17847535469.9%

반응 조건

온도50 °C

반응 단계

1-(6-Acetoxynaphthalen-2-yl)-1-(1-trityl-1H-imidazol-4-yl)-2-methyl-1-propanol (0.25 g) was dissolved in acetic acid (20 ml). To the mixture was added 10% palladium carbon (0.1 g). The mixture was stirred at 50° C. for 2 h under hydrogen atmosphere. The catalyst was filtered off, and filtrate was concentrated. The residue was purified by silica gel chromatography (eluent; dichloromethane-methanol=10:1) to give the titled compound (0.1 g) as a colorless solid.

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US06573289B1
출처 데이터셋uspto-grants-2003_06
ORD IDord-294df26305144dcbba769b9e9633acc5
출처 메모uspto-grants-2003_06