참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Triethylamine | HCID 8471 | — |
| 반응물 | Methacryloyl chloride | HCID 13528 | — |
| 반응물 | 2-Ethyl-2-adamantanol | HCID 4401951 | — |
| 용매 | Methyl Isobutyl Ketone | HCID 7909 | — |
| 생성물 | 2-Ethyl-2-methacryloyloxyadamantane | HCID 9813645 | 60% |
반응 단계
180 g of 2-Ethyl-2-adamantanol, 303 g of triethylamine and 500 g of methylisobutyl ketone were mixed by stirring at 90° C. While stirring, 157 g of methacrylic acid chloride was added dropwise to the mixture. After completion of the dropwise addition, the mixture was further stirred for 72 hours. Then, extraction and distillation were conducted to obtain 2-ethyl-2-adamantyl methacrylate at the yield of 60%.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US06579659B2 |
|---|
| 출처 데이터셋 | uspto-grants-2003_06 |
|---|
| ORD ID | ord-9a8617f7ceab4cba9d7d1e46a274944a |
|---|
| 출처 메모 | uspto-grants-2003_06 |
|---|
