Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Isopropenyl acetate → (+)-Styrallyl acetate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Isopropenyl acetate | HCID 7916 | — |
| 반응물 | 4-Chlorophenyl Acetate | HCID 13410 | — |
| 생성물 | (+)-Styrallyl acetate | HCID 6951704 | 95% |
반응 단계
The procedure of Example 1 was repeated except that 3 molar equivalents of p-chlorophenyl acetate (a conventional acylating agent) was used in place of isopropenyl acetate in the presence of three times the amount of the enzyme catalyst used in Example 1 over a reaction period of 42 hours, to obtain (R)-1-phenylethyl acetate having an optical purity of higher than 99%, at a yield of 95%.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07156731B2 |
| 출처 데이터셋 | uspto-grants-2007_01 |
| ORD ID | ord-1bc0273f6d9e4898b5a2d888224182f6 |
| 출처 메모 | uspto-grants-2007_01 |