Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2,6-Dichloro-4-isocyanatopyridine → N-{[4-(3,4-Dichlorobenzyl)morpholin-2-yl]methyl}N'-(2,6-dichloropyridin-4-yl)urea
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2,6-Dichloro-4-isocyanatopyridine | HCID 2781658 | — |
| 반응물 | [4-(3,4-Dichlorobenzyl)morpholin-2-yl]methylamine | HCID 10308229 | — |
| 생성물 | N-{[4-(3,4-Dichlorobenzyl)morpholin-2-yl]methyl}N'-(2,6-dichloropyridin-4-yl)urea | HCID 10183254 | 39.1% |
반응 단계
Example 24 was prepared in an analogous manner to Example 1 using a mixture of Intermediate 3 (0.025 g) and 2,6-dichloro-4-isocyanatopyridine (0.0258 g) to give the title compound (0.0165 g). LC-MS (System A): Rt 2.46 mins, Mass Spectrum m/z 463 [MH+].
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07157457B2 |
| 출처 데이터셋 | uspto-grants-2007_01 |
| ORD ID | ord-fb45000ffe6b4b209ec323ca48bb05f5 |
| 출처 메모 | uspto-grants-2007_01 |