Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Hydrazine → 4'-Hydrazino-2,2':6',2''-terpyridine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Hydrazine | HCID 9321 | — |
| 반응물 | 4'-Chloro-2,2':6',2''-terpyridine | HCID 667748 | — |
| 용매 | (+-)-2-Butanol | HCID 6568 | — |
| 생성물 | 4'-Hydrazino-2,2':6',2''-terpyridine | HCID 10539488 | — |
반응 단계
4 ml (126 mmol) of hydrazine are added to 600 mg (2.2 mmol) of 4′-chloro-[2,2′;6′,2″]-terpyridine in 12 ml of 2-butanol. The mixture is heated at reflux for 17 hours and cooled, and [2,2′;6′,2″]terpyridin-4′-yl-hydrazine is filtered off in the form of a white solid.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07161005B2 |
| 출처 데이터셋 | uspto-grants-2007_01 |
| ORD ID | ord-8f26a72bb9c44fd3b9a732bd32cb2f68 |
| 출처 메모 | uspto-grants-2007_01 |