Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Thionyl Chloride → Di(pentafluorophenyl)dichlorosilane
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Thionyl Chloride | HCID 24386 | — |
| 반응물 | Bis(pentafluorophenyl)diethoxysilane | HCID 11102434 | — |
| 반응물 | Pyridinium hydrochloride | HCID 21584435 | — |
| 생성물 | Di(pentafluorophenyl)dichlorosilane | HCID 11112867 | — |
반응 단계
180.93 g (0.400 mol) di(pentafluorophenyl)diethoxysilane, 146 mL (2.00 mol, 237.9 g) thionylchloride and 4.92 g (0.0426 mol) pyridinium hydrochloride are refluxed and stirred for 16 h. Excess of SOCl2 is evaporated and di(pentafluorophenyl)dichlorosilane isolated by vacuum-distillation.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07161019B2 |
| 출처 데이터셋 | uspto-grants-2007_01 |
| ORD ID | ord-b33d27536ce4471892c0cbe98ee0b606 |
| 출처 메모 | uspto-grants-2007_01 |