tert-butyl (4R)-4-{[(benzyloxy)carbonyl]amino}pentanoate → HCID 58781983, 화합물
반응식
C(OC([NH:11][C@H:12]([CH3:22])[CH2:13][CH2:14][C:15]([O:17][C:18]([CH3:21])([CH3:20])[CH3:19])=[O:16])=O)C1C=CC=CC=1>CO.[Pd]>[NH2:11][C@H:12]([CH3:22])[CH2:13][CH2:14][C:15]([O:17][C:18]([CH3:21])([CH3:20])[CH3:19])=[O:16]참가 물질
4
실험 절차
To a solution of tert-butyl (4R)-4-{[(benzyloxy)carbonyl]amino}pentanoate (3.5 g, 11.4 mmol) in methanol (35 ml) was added Pd—C (0.7 g) and the mixture was stirred under a hydrogen atomosphere for 3 hours. Catalyst was-removed by filtration and the solvent was removed in vacuo to give tert-butyl(4R)-4-aminopentanoate (2.1 g).
후처리
- customCatalyst was-removed by filtration
- customthe solvent was removed in vacuo
출처 및 근거
- ORD 기록
- ord-62a1634cec9145a4826dd171d59b7ea3
- 출처 데이터셋
- uspto-grants-2007_01
- 특허 번호
- US07163936B2
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