Methylamine → HCID 21077593, 화합물

HRID 1374646노트

반응식

HRID 1374646 반응식
[CH3:1][S:2][C:3]1[N:8]=[C:7](Cl)[C:6]([O:10][CH3:11])=[CH:5][N:4]=1.[CH3:12][NH2:13].C1CCCCC1.C(OCC)(=O)C>C(O)C>[CH3:1][S:2][C:3]1[N:8]=[C:7]([NH:13][CH3:12])[C:6]([O:10][CH3:11])=[CH:5][N:4]=1

참가 물질

5

반응물 3

HCID 6329MethylamineHCID 2435114-Chloro-5-methoxy-2-(methylsulfanyl)pyrimidineHCID 21867204Cyclohexane ethylacetate

생성물 1

HCID 21077593HCID 21077593, 화합물

시약·촉매·용매 1

HCID 702Ethanol용매

실험 절차

Prepared from 2-methylsulphenyl-4-chloro-5-methoxy-pyrimidine by reacting with methylamine in ethanol at 90° C., Rf value: 0.22 (silica gel; cyclohexane/ethyl acetate=2:1)

출처 및 근거

ORD 기록
ord-f9e56a004e814f4ab48b651c6fa6e567
출처 데이터셋
uspto-grants-2007_01
특허 번호
US07166599B2

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