Methylamine → HCID 241191, 화합물

HRID 1374647노트

반응식

HRID 1374647 반응식
[CH3:1][S:2][C:3]1[N:8]=[C:7](Cl)[C:6]([CH3:10])=[CH:5][N:4]=1.[CH3:11][NH2:12].C(Cl)Cl.CO>C(O)C>[CH3:1][S:2][C:3]1[N:8]=[C:7]([NH:12][CH3:11])[C:6]([CH3:10])=[CH:5][N:4]=1

참가 물질

5

반응물 3

HCID 6329MethylamineHCID 21226129Dichloromethane methanolHCID 235627084-Chloro-5-methyl-2-(methylthio)pyrimidine

생성물 1

HCID 241191HCID 241191, 화합물

시약·촉매·용매 1

HCID 702Ethanol용매

실험 절차

Prepared from 2-methylsulphenyl-4-chloro-5-methyl-pyrimidine by reacting with methylamine in ethanol at 100° C., melting point: 134° C., Rf value: 0.35 (silica gel; methylene chloride/methanol=40:1)

출처 및 근거

ORD 기록
ord-33e661c97a374a4ba36280217621b54d
출처 데이터셋
uspto-grants-2007_01
특허 번호
US07166599B2

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