Methanol → Methyl 3,5-dichloro-4-methylbenzoate

반응식

[Cl:1][C:2]1[CH:3]=[C:4]([CH:8]=[C:9]([Cl:12])[C:10]=1[CH3:11])[C:5]([OH:7])=[O:6].[CH3:13]O>>[Cl:1][C:2]1[CH:3]=[C:4]([CH:8]=[C:9]([Cl:12])[C:10]=1[CH3:11])[C:5]([O:7][CH3:13])=[O:6]

참가 물질

반응물 2

HCID 887Methanol

HCID 185332343,5-Dichloro-4-methylbenzoic acid

생성물 1

HCID 10130655Methyl 3,5-dichloro-4-methylbenzoate

실험 절차

This compound was prepared in the same manner as in Reference Example 1 (step 1), except that 3,5-dichloro-4-methylbenzoic acid (Japanese Unexamined Patent Publication (Kokai) No. 6-192196) was used and methanol was used as the solvent, and that the crude product was purified by silica gel column chromatography.

후처리

customthat the crude product was purified by silica gel column chromatography

출처 및 근거

ORD 기록: ord-e51b2b92542745ac848a958d9fc03db1
출처 데이터셋: uspto-grants-2010_06
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US07728131B2

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