4,5-Diphenylimidazole → 2-(2-Methoxyethoxy)ethyl 8-(4,5-diphenylimidazole-1-yl)octanoate

HRID 1376345

반응식

HRID 1376345 반응식
[C:1]1([C:7]2[N:8]=[CH:9][NH:10][C:11]=2[C:12]2[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=2)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.Br[CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][C:26]([O:28][CH2:29][CH2:30][O:31][CH2:32][CH2:33][O:34][CH3:35])=[O:27]>>[C:1]1([C:7]2[N:8]=[CH:9][N:10]([CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][C:26]([O:28][CH2:29][CH2:30][O:31][CH2:32][CH2:33][O:34][CH3:35])=[O:27])[C:11]=2[C:12]2[CH:13]=[CH:14][CH:15]=[CH:16][CH:17]=2)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1

참가 물질

3

반응물 2

HCID 695884,5-DiphenylimidazoleHCID 229164492-(2-Methoxy-ethoxy)ethyl 8-bromooctanoate

생성물 1

HCID 229163602-(2-Methoxyethoxy)ethyl 8-(4,5-diphenylimidazole-1-yl)octanoate

실험 절차

4,5-Diphenylimidazole (2.85 g) was treated with 2-(2-methoxy-ethoxy)ethyl 8-bromooctanoate (8.63 g) as described in Example 20 to give 2-(2-methoxyethoxy)ethyl 8-(4,5-diphenylimidazole-1-yl)octanoate as a colourless oil (i.5 g, 25%). Found: C, 72.28; H, 7.91; N, 6.35% C28H36N2O4 requires: C, 72.38; H, 7.81; N, 6.03%

출처 및 근거

ORD 기록
ord-74dde27a96ae4c93a024ebb30c9700ad
출처 데이터셋
uspto-grants-1997_09
특허 번호
US05663053

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