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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 1377655생성일: 2026년 10월 26일

(Z)-2-[3-[4-[2-(5-methyl-2-phenyl-4-oxazolyl)ethoxy]phenyl]-2-propenyl]-1,3-dioxane → 2-[3-[4-[2-(5-Methyl-2-phenyl-4-oxazolyl)ethoxy]phenyl]propyl]-1,3-dioxane

https://huagongshe.com/reaction/1377655

반응식

참여 물질

역할이름HCID투입량
반응물(Z)-2-[3-[4-[2-(5-methyl-2-phenyl-4-oxazolyl)ethoxy]phenyl]-2-propenyl]-1,3-dioxaneHCID 11811571—
촉매HCID 178418390HCID 178418390—
용매EthanolHCID 702—
생성물2-[3-[4-[2-(5-Methyl-2-phenyl-4-oxazolyl)ethoxy]phenyl]propyl]-1,3-dioxaneHCID 1102590296%

반응 단계

A mixture of (Z)-2-[3-[4-[2-(5-methyl-2-phenyl-4-oxazolyl)ethoxy]phenyl]-2-propenyl]-1,3-dioxane (5.0 g), palladium-carbon (5%, 0.1 g) and ethanol (100 ml) was subjected to catalytic hydrogenation at room 5 temperature under one atmospheric pressure. The catalyst was filtered off, and the filtrate was concentrated under reduced pressure. The concentrate was purified by means of a silica gel column chromatography. From the fractions eluted with hexane--ethyl acetate (1:1), 2-[3-[4-[2-(5-methyl-2-phenyl-4-oxazolyl)ethoxy]phenyl]propyl]-1,3-dioxane (4.8 g, 96%) was obtained.

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US05665748
출처 데이터셋uspto-grants-1997_09
ORD IDord-b6bf045aeb2148a1b4b3c030cdc2e274
출처 메모uspto-grants-1997_09