Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Benzyl Bromide → N-benzyl-N-(1,2,2,6,6-pentamethylpiperidin-4-yl)hydroxylamine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Benzyl Bromide | HCID 7498 | — |
| 반응물 | 1,2,2,6,6-Pentamethyl-piperidin-4-one oxime | HCID 241950 | — |
| 생성물 | N-benzyl-N-(1,2,2,6,6-pentamethylpiperidin-4-yl)hydroxylamine | HCID 22902720 | 40% |
반응 단계
Following the procedure of Example 1, the title compound is prepared from 1,2,2,6,6-pentamethylpiperidin-4-one oxime (5.0 g, 27 mmol) and benzyl bromide (4.6 g, 27 mmol) in a 40% yield to give 3.0 g of a white solid which melts at 107°-108° C. after recrystallization from ethanol.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05668198 |
| 출처 데이터셋 | uspto-grants-1997_09 |
| ORD ID | ord-8b77997329644ab3846141c875533c57 |
| 출처 메모 | uspto-grants-1997_09 |