m-Chloroperbenzoic acid → 86088-36-0
반응식
[C:1]1([CH2:7][CH2:8][CH2:9][CH:10]=[CH2:11])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.ClC1C=CC=C(C(OO)=[O:20])C=1>ClCCl>[C:1]1([CH2:7][CH2:8][CH2:9][CH:10]2[CH2:11][O:20]2)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1참가 물질
4
실험 절차
5-Phenylpent-1-ene (14.2 g, 0.0973 mol) and m-chloroperbenzoic acid (16.79 g, 0.0973 mol) in dichloromethane (300 ml) was stirred at room temperature for 4 hours. The solution was washed with saturated aqueous sodium hydrogen carbonate solution and dried (MgSO4). The solvent was evaporated off under reduced pressure to give an oil which was distilled to give 2-(3-phenylpropyl)oxirane (b.p. 85° C., 0.4 mm.Hg).
후처리
- washThe solution was washed with saturated aqueous sodium hydrogen carbonate solution
- dry with materialdried (MgSO4)
- customThe solvent was evaporated off under reduced pressure
- customto give an oil which
- distillationwas distilled
출처 및 근거
- ORD 기록
- ord-205a8488e9cc4405b1ddfb57e7330eaa
- 출처 데이터셋
- uspto-grants-1986_04
- 특허 번호
- US04579862
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