Ethyl 3-phenylprop-2-enoate → Oetfvkzgqqiumv-uhfffaoysa-

HRID 1380157노트

반응식

HRID 1380157 반응식
[Cl:1][GeH:2]([Cl:4])[Cl:3].[C:5]([O:15][CH2:16][CH3:17])(=[O:14])[CH:6]=[CH:7][C:8]1[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=1>>[Cl:1][Ge:2]([Cl:4])([Cl:3])[CH:7]([C:8]1[CH:9]=[CH:10][CH:11]=[CH:12][CH:13]=1)[CH2:6][C:5]([O:15][CH2:16][CH3:17])=[O:14]

참가 물질

3

반응물 2

HCID 7649Ethyl 3-phenylprop-2-enoateHCID 70900CID 70900

생성물 1

HCID 13335372Oetfvkzgqqiumv-uhfffaoysa-수율 78.7%

실험 절차

A mixture of 36 g (0.2 mol) of trichlorogermane and 35.2 g (0.2 mol) of ethyl cinnamate was stirred for 2 hours, and then the reaction product was distilled under vacuum to afford 56 g of a fraction, b.p. 169°-170° C./4 mmHg. Yield 78.7%.

후처리

  1. distillationthe reaction product was distilled under vacuum
  2. customto afford 56 g of a fraction, b.p. 169°-170° C./4 mmHg

출처 및 근거

ORD 기록
ord-b7fb6a81bde4472f926d23b60de8a565
출처 데이터셋
uspto-grants-1986_04
특허 번호
US04579961

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