Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-Ethenylbenzenesulfonamide → N-[(4,6-Dichloro-1,3,5-triazin-2-yl)aminocarbonyl]-2-ethenylbenzenesulfonamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-Ethenylbenzenesulfonamide | HCID 11367403 | — |
| 반응물 | 2,4-Dichloro-6-isocyanato-1,3,5-triazine | HCID 13052624 | — |
| 용매 | Acetonitrile | HCID 6342 | — |
| 생성물 | N-[(4,6-Dichloro-1,3,5-triazin-2-yl)aminocarbonyl]-2-ethenylbenzenesulfonamide | HCID 20218271 | — |
반응 단계
A solution of 4,6-dichloro-1,3,5-triazin-2-yl isocyanate (0.87 g, 4.5 mmol) in acetonitrile (9 ml) is contacted with 2-ethenylbenzenesulfonamide (0.83 g, 4.5 mmol) and stirred for 16 hours. The mixture is then evaporated under reduced pressure to yield the title compound which is used directly in subsequent reactions.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04582525 |
| 출처 데이터셋 | uspto-grants-1986_04 |
| ORD ID | ord-1656e35c0a6340cfb2e723df0ac630a5 |
| 출처 메모 | uspto-grants-1986_04 |