N,N-Dimethylethylenediamine → HCID 13590121, 화합물

반응식

Cl[C:2]1[C:15]2[C:14](=[O:16])[C:13]3[C:8](=[CH:9][CH:10]=[C:11]([OH:17])[CH:12]=3)[S:7][C:6]=2[C:5]([N+:18]([O-:20])=[O:19])=[CH:4][CH:3]=1.[CH3:21][N:22]([CH3:26])[CH2:23][CH2:24][NH2:25]>>[CH3:21][N:22]([CH3:26])[CH2:23][CH2:24][NH:25][C:2]1[C:15]2[C:14](=[O:16])[C:13]3[C:8](=[CH:9][CH:10]=[C:11]([OH:17])[CH:12]=3)[S:7][C:6]=2[C:5]([N+:18]([O-:20])=[O:19])=[CH:4][CH:3]=1

참가 물질

반응물 2

HCID 66053N,N-Dimethylethylenediamine

HCID 135901181-Chloro-7-hydroxy-4-nitro-9H-thioxanthen-9-one

생성물 1

HCID 13590121HCID 13590121, 화합물

실험 절차

1-[[2-(Dimethylamino)ethyl]amino]-7-hydroxy-4-nitro-9H-thioxanthen-9-one was prepared similarly from 10 g of 1-chloro-7-hydroxy-4-nitrothioxanthone and 5.7 g of N,N-dimethylethylenediamine to provide 7.2 g, mp>300°.

후처리

customto provide 7.2 g, mp>300°

출처 및 근거

ORD 기록: ord-954b4cf3d0b7416e98a2a7f30bbac196
출처 데이터셋: uspto-grants-1986_04
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US04582851

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