Dimethylthiocarbamoyl chloride → HCID 53894584, 화합물

HRID 1380836노트

반응식

HRID 1380836 반응식
[Cl:1][CH2:2][C:3]1[CH:8]=[C:7]([OH:9])[N:6]=[C:5]([CH3:10])[N:4]=1.[CH3:11][N:12]([CH3:16])[C:13](Cl)=[S:14]>>[CH3:11][N:12]([CH3:16])[C:13](=[S:14])[O:9][C:7]1[N:6]=[C:5]([CH3:10])[N:4]=[C:3]([CH2:2][Cl:1])[CH:8]=1

참가 물질

3

반응물 2

HCID 27871Dimethylthiocarbamoyl chlorideHCID 178433451HCID 178433451, 화합물

생성물 1

HCID 53894584HCID 53894584, 화합물

실험 절차

4-Chloromethyl-6-hydroxy-2-methyl-pyrimidine is reacted with N,N-dimethylthiocarbamoyl chloride analogously to the process described in Example 86 in order to produce 4-chloromethyl-2-methyl-6-pyrimidinyl N,N-dimethylthiocarbamate which is required as the starting material in Example 30. This product is obtained in the form of a yellow oil.

출처 및 근거

ORD 기록
ord-4da97e024df44118840f5afe7034730c
출처 데이터셋
uspto-grants-1986_04
특허 번호
US04584295

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