3-Chloro-1,1-diethoxypropane → 3-(7,8-Dimethoxy-1,3-dihydro-2H-3-benzazepin-2-on-3-yl)-propionaldehyde diethylacetal

HRID 1380865

반응식

HRID 1380865 반응식
[CH3:1][O:2][C:3]1[C:14]([O:15][CH3:16])=[CH:13][C:6]2[CH2:7][C:8](=[O:12])[NH:9][CH:10]=[CH:11][C:5]=2[CH:4]=1.[CH2:17]([O:19][CH:20]([O:24][CH2:25][CH3:26])[CH2:21][CH2:22]Cl)[CH3:18]>>[CH2:17]([O:19][CH:20]([O:24][CH2:25][CH3:26])[CH2:21][CH2:22][N:9]1[C:8](=[O:12])[CH2:7][C:6]2[CH:13]=[C:14]([O:15][CH3:16])[C:3]([O:2][CH3:1])=[CH:4][C:5]=2[CH:11]=[CH:10]1)[CH3:18]

참가 물질

3

반응물 2

HCID 962173-Chloro-1,1-diethoxypropaneHCID 14823731,3-Dihydro-7,8-dimethoxy-2H-3-benzazepin-2-one

생성물 1

HCID 135796433-(7,8-Dimethoxy-1,3-dihydro-2H-3-benzazepin-2-on-3-yl)-propionaldehyde diethylacetal

실험 절차

This is prepared analogously to Example H (a) by reacting 7,8-dimethoxy-1,3-dihydro-2H-3-benzazepin-2-one with 3-chloro-propionaldehyde diethyl acetal.

출처 및 근거

ORD 기록
ord-0bac11497e74453aa094882276f0ef53
출처 데이터셋
uspto-grants-1986_04
특허 번호
US04584293

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