Triethylamine → HCID 23323498, 화합물

HRID 1381132노트

반응식

HRID 1381132 반응식
[N+:1]([C:4]1[CH:5]=[C:6]([NH:10][C:11]2[CH:19]=[CH:18][CH:17]=[CH:16][C:12]=2[C:13]([NH2:15])=O)[CH:7]=[CH:8][CH:9]=1)([O-:3])=[O:2].C(N(CC)CC)C>>[N+:1]([C:4]1[CH:5]=[C:6]([NH:10][C:11]2[CH:19]=[CH:18][CH:17]=[CH:16][C:12]=2[C:13]#[N:15])[CH:7]=[CH:8][CH:9]=1)([O-:3])=[O:2]

참가 물질

3

반응물 2

HCID 8471TriethylamineHCID 54259173HCID 54259173, 화합물

생성물 1

HCID 23323498HCID 23323498, 화합물

실험 절차

3,85 g (15 mMol) of 2-(3-Nitrophenylamino)benzoic acid amide in 30 ml (0,325 Mol) phosphorooxychloride were treated with 4,32 ml (31 mMol) triethylamine which is added dropwise, whereby the reaction mixture warms up. After thirty minutes the excess of phosphorooxychloride is distilled off, the residue is treated with water and the solid product is filtered off.

후처리

  1. additionis added dropwise
  2. distillationAfter thirty minutes the excess of phosphorooxychloride is distilled off
  3. additionthe residue is treated with water
  4. filtrationthe solid product is filtered off

출처 및 근거

ORD 기록
ord-9169ece5721a40f1a816b90af66ae9d8
출처 데이터셋
uspto-grants-1986_04
특허 번호
US04585772

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