Potassium Hydroxide → HCID 12330022, 화합물

반응식

[Cl:1][C:2]1[CH:21]=[CH:20][CH:19]=[C:18]([C:22]([O:24]CC)=[O:23])[C:3]=1[CH2:4][O:5][C:6]1[CH:11]=[CH:10][C:9]([CH2:12][C:13]([O:15]CC)=[O:14])=[CH:8][CH:7]=1.[OH-].[K+]>>[C:22]([C:18]1[CH:19]=[CH:20][CH:21]=[C:2]([Cl:1])[C:3]=1[CH2:4][O:5][C:6]1[CH:7]=[CH:8][C:9]([CH2:12][C:13]([OH:15])=[O:14])=[CH:10][CH:11]=1)([OH:24])=[O:23]

참가 물질

반응물 2

HCID 14797Potassium Hydroxide

HCID 21269134Ethyl 4-(2-chloro-6-ethoxycarbonylbenzyloxy)phenylacetate

생성물 1

HCID 12330022HCID 12330022, 화합물

실험 절차

Reaction of ethyl 4-(2-chloro-6-ethoxycarbonylbenzyloxy)phenylacetate with potassium hydroxide as described in Example 1c provides 4-(2-carboxy-6-chlorobenzyloxy)phenylacetic acid as a colorless solid, m.p. 171°-173° C.

출처 및 근거

ORD 기록: ord-096f10f5e9ce43d1ad0c5b5f6bd4e709
출처 데이터셋: uspto-grants-1986_04
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US04585788

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