참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Ethoxyethylamine | HCID 66970 | — |
| 반응물 | (R,R)-Stilbene oxide | HCID 185583 | — |
| 생성물 | beta-[(2-Ethoxyethyl)amino]-alpha-phenylbenzeneethanol | HCID 14391209 | 80% |
반응 단계
A mixture of trans-stilbene oxide (1.96 g, 0.010 mole) and 2-ethoxyethylamine (2.67 g, 0.030 mole) was heated at 140° C. for 6 hours. After standing at ambient temperature for 10 hours, the solidified reaction mixture was triturated with isooctane and filtered to give 2.28 g of white solid (80%) which was recrystallized from isooctane, m.p. 128°-130° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US04803200 |
|---|
| 출처 데이터셋 | uspto-grants-1989_02 |
|---|
| ORD ID | ord-a6e5a8d6ef254ec6b2534898854e9dca |
|---|
| 출처 메모 | uspto-grants-1989_02 |
|---|
