HCID 21276215, 화합물 → (10-Bromo-1-anthracenyl)methanol

HRID 1381736노트

반응식

HRID 1381736 반응식
[Br:1][C:2]1[C:15]2[C:10](=[CH:11][CH:12]=[CH:13][CH:14]=2)[CH:9]=[C:8]2[C:3]=1[CH:4]=[CH:5][CH:6]=[C:7]2[C:16](O)=[O:17]>C1COCC1>[Br:1][C:2]1[C:15]2[C:10](=[CH:11][CH:12]=[CH:13][CH:14]=2)[CH:9]=[C:8]2[C:3]=1[CH:4]=[CH:5][CH:6]=[C:7]2[CH2:16][OH:17]

참가 물질

3

반응물 1

HCID 21276215HCID 21276215, 화합물

생성물 1

HCID 13375398(10-Bromo-1-anthracenyl)methanol

시약·촉매·용매 1

HCID 8028Tetrahydrofuran용매

실험 절차

10-Bromo-1-anthracenecarboxylic acid made from example 2B by the procedure of E. Barnett, J. W. Cook, and H. H. Grainger, Ber. 57 B, 1775 (1924), was reduced with BH3 in THF by the procedure outlined in 2C to give (10-bromo-1-anthryl)methanol mp 125°-127°, (EtOAc/hexane), (C, H, Br).

출처 및 근거

ORD 기록
ord-718dafb78e014ff585704365454bdb82
출처 데이터셋
uspto-grants-1989_02
특허 번호
US04803226

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