(10-Bromo-1-anthracenyl)methanol → HCID 14370037, 화합물

HRID 1381737노트

반응식

HRID 1381737 반응식
[Br:1][C:2]1[C:15]2[C:10](=[CH:11][CH:12]=[CH:13][CH:14]=2)[CH:9]=[C:8]2[C:3]=1[CH:4]=[CH:5][CH:6]=[C:7]2[CH2:16][OH:17].C1C=C[NH+]=CC=1.[O-][Cr](Cl)(=O)=O>>[Br:1][C:2]1[C:15]2[C:10](=[CH:11][CH:12]=[CH:13][CH:14]=2)[CH:9]=[C:8]2[C:3]=1[CH:4]=[CH:5][CH:6]=[C:7]2[CH:16]=[O:17]

참가 물질

3

반응물 2

HCID 13375398(10-Bromo-1-anthracenyl)methanolHCID 178418287HCID 178418287, 화합물

생성물 1

HCID 14370037HCID 14370037, 화합물

실험 절차

Using the procedure outlined in 2D, oxidation of (10-bromo-1-anthryl)-methanol with PCC gave 10-bromo-1-anthracenecarbaldehyde mp 134.5°-135.5°, (PhCH3 /hexane), (C, H, Br).

출처 및 근거

ORD 기록
ord-09caf993845f4098942240615f2dfb49
출처 데이터셋
uspto-grants-1989_02
특허 번호
US04803226

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