HCID 178471920, 화합물 → 3-benzoyl-8-methoxy-4(1H)-quinolone
반응식
[C:1]([C:9](=[CH:15][NH:16][C:17]1[CH:22]=[CH:21][CH:20]=[CH:19][C:18]=1[O:23][CH3:24])[C:10]([O:12]CC)=O)(=[O:8])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1>C1(OC2C=CC=CC=2)C=CC=CC=1>[C:1]([C:9]1[C:10](=[O:12])[C:22]2[C:17](=[C:18]([O:23][CH3:24])[CH:19]=[CH:20][CH:21]=2)[NH:16][CH:15]=1)(=[O:8])[C:2]1[CH:3]=[CH:4][CH:5]=[CH:6][CH:7]=1참가 물질
3
실험 절차
Ethyl 2-benzoyl-3-(2-methoxyphenylamino)acrylate (6.0 g, 0.018 mol) was added in portions to boiling diphenyl ether (100 ml) and heated under reflux for 45 minutes. The reaction mixture was allowed to cool and diluted with petroleum ether to afford the crystalline 3-benzoyl-8-methoxy-4(1H)-quinolone (4.7 g, 91%).
후처리
- temperatureheated
- temperatureunder reflux for 45 minutes
- temperatureto cool
출처 및 근거
- ORD 기록
- ord-3ca8a8a59adb420eb4fefa3c6892f6d9
- 출처 데이터셋
- uspto-grants-1989_02
- 특허 번호
- US04806549
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