Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Benzamide, N-cyano- → HCID 178512389, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Benzamide, N-cyano- | HCID 84805 | — |
| 반응물 | 4-Amino-1-(2-naphthyl)methylpiperidine | HCID 11195823 | — |
| 용매 | Toluene | HCID 1140 | — |
| 생성물 | HCID 178512389 | HCID 178512389 | 40.4% |
반응 단계
4-Amino-1-(naphth-2-ylmethyl)piperidine (1.0 g, 0.0042 m) and benzoyl cyanamide (0.67 g, 0.0042 m) in toluene (100 cm3) were refluxed for 15 hours. The solvent was evaporated and the residue recrystallised from the minimum amount of isopropyl alcohol and recrystallised twice more from ethanol to give 0.65 g of the title compound, m.p. dihydrochloride quarter hydrate, m.p. 260°-262° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04806552 |
| 출처 데이터셋 | uspto-grants-1989_02 |
| ORD ID | ord-8dae87f3430247cfba9c9f42b16f3681 |
| 출처 메모 | uspto-grants-1989_02 |