Lauric Acid → N-(2-Methoxy-5-pyridyl)-cyclopropane carboxamide dodecanoic acid salt

HRID 1382775

반응식

HRID 1382775 반응식
[CH3:1][O:2][C:3]1[CH:8]=[CH:7][C:6]([NH:9][C:10]([CH:12]2[CH2:14][CH2:13]2)=[O:11])=[CH:5][N:4]=1.[C:15]([OH:28])(=[O:27])[CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH3:26]>CC(C)=O>[C:15]([OH:28])(=[O:27])[CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH3:26].[CH3:1][O:2][C:3]1[CH:8]=[CH:7][C:6]([NH:9][C:10]([CH:12]2[CH2:14][CH2:13]2)=[O:11])=[CH:5][N:4]=1

참가 물질

4

반응물 2

HCID 3893Lauric AcidHCID 86308N-(6-methoxypyridin-3-yl)cyclopropanecarboxamide

생성물 1

HCID 14304482N-(2-Methoxy-5-pyridyl)-cyclopropane carboxamide dodecanoic acid salt

시약·촉매·용매 1

HCID 180Acetone용매

실험 절차

Three grams (0.016 mole) of the compound of Example 1 was dissolved in 100 ml of acetone in a 300 ml, one-neck, round-bottom flask by swirling. 3.2 g (0.016 mole) dodecanoic acid was added which went into solution. The resulting solution was evaporated on a rotary evaporator, yielding 6.2 g, of a white solid having a melting point of 92°-96° C., which was identified by nuclear magnetic resonance spectroscopy as the title compound. This compound will be known as Compound 7.

후처리

  1. customThe resulting solution was evaporated on a rotary evaporator
  2. customyielding 6.2 g

출처 및 근거

ORD 기록
ord-9c9bfa754a764e7db319a08e61b9d8a8
출처 데이터셋
uspto-grants-1989_02
특허 번호
US04808600

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