Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Isovaleryl chloride → N-(6-(2,4-dichlorophenyl)-5-(4-chlorophenyl)-3-cyanopyridin-2-yl)-N,3-dimethylbutanamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Isovaleryl chloride | HCID 66054 | — |
| 반응물 | 6-(2,4-Dichlorophenyl)-5-(4-chlorophenyl)-2-(methylamino)pyridine-3-carbonitrile | HCID 68719045 | — |
| 반응물 | HCID 178418689 | HCID 178418689 | — |
| 생성물 | N-(6-(2,4-dichlorophenyl)-5-(4-chlorophenyl)-3-cyanopyridin-2-yl)-N,3-dimethylbutanamide | HCID 68717246 | — |
반응 단계
The product of Step D Example 1 was reacted with MeMgBr followed by 3-methylbutanoyl chloride using the procedure of EXAMPLE 42 Step A to afford the title compound. HPLC/MS: 472.2 (M+1), 474.2 (M+3); Rt=4.43 min.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07728141B2 |
| 출처 데이터셋 | uspto-grants-2010_06 |
| ORD ID | ord-f77414101d6f4d47b45db786e34fd591 |
| 출처 메모 | uspto-grants-2010_06 |