HCID 21273330, 화합물 → HCID 14372147, 화합물

HRID 1382999노트

반응식

HRID 1382999 반응식
S([C:5]1[O:13][C:12]2[CH:11]=[C:10](C)[NH:9][C:8](=[O:15])[C:7]=2[CH:6]=1)(=O)(=O)N.O1C=CC=[C:17]1C(C)=CC(O)=O.O1C=CC=C1C=C(C)C(O)=O>>[CH3:17][C:11]1[C:12]2[O:13][CH:5]=[CH:6][C:7]=2[C:8](=[O:15])[NH:9][CH:10]=1

참가 물질

4

반응물 3

HCID 21273330HCID 21273330, 화합물HCID 538068063-(2-Furanyl)methacrylic acidHCID 54212216HCID 54212216, 화합물

생성물 1

HCID 14372147HCID 14372147, 화합물

실험 절차

The title compound was prepared according to the procedure described for 2-sulfamoyl-6-methylfuro[3.2-c]pyridin-4-(5H)-one (Example 12 Step A) except 3-(2-furanyl)-3-methylacrylic acid was substituted for 3-(2-furanyl)methacrylic acid. Title compound was obtained in 41% yield, m.p. 239°-241° C., after crystallization from methanol.

후처리

  1. customThe title compound was prepared

출처 및 근거

ORD 기록
ord-883d592244404fceadbf46d0f3f1ab4a
출처 데이터셋
uspto-grants-1989_02
특허 번호
US04808595

반응 노트

불러오는 중…