Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Phenanthrene-9-carbaldehyde → 2-Ethoxymethyl-2-(((9-phenanthrenyl)methyl)amino)-1,3-propanediol hydrochloride
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Phenanthrene-9-carbaldehyde | HCID 78437 | — |
| 반응물 | 2-Amino-2-ethoxymethyl-1,3-propanediol hydrochloride | HCID 15599336 | — |
| 반응물 | (+-)(2R*,3S*)-2-((9-Phenanthrenylmethyl)amino)-2-methyl-1,3-butanediol hydrochloride | HCID 86741971 | — |
| 생성물 | 2-Ethoxymethyl-2-(((9-phenanthrenyl)methyl)amino)-1,3-propanediol hydrochloride | HCID 21273664 | — |
반응 단계
Using the reductive amination procedure outlined for 7G, phenanthrene-9-carbaldehyde (Aldrich) and 2-amino-2-ethoxymethyl-1,3-propanediol hydrochloride.1/4H2O (8B) gave 2-ethoxymethyl-2-(((9-phenanthrenyl)methyl)amino)-1,3-propanediol hydrochloride mp 173°-175°, (EtOH/Et2O), (C, H, Cl, N).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04808625 |
| 출처 데이터셋 | uspto-grants-1989_02 |
| ORD ID | ord-2d3f18eec6094fc68773a16b800e3f2b |
| 출처 메모 | uspto-grants-1989_02 |