돌아가기
Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 1383040생성일: 2026년 10월 26일

Phenanthrene-9-carbaldehyde → 3-Methoxy-2-methyl-2-((9-phenanthrenylmethyl)amino)-1-propanol hydrochloride

https://huagongshe.com/reaction/1383040

반응식

참여 물질

역할이름HCID투입량
반응물Phenanthrene-9-carbaldehydeHCID 78437—
반응물2-Amino-3-methoxy-2-methylpropan-1-olHCID 13375415—
반응물(+-)(2R*,3S*)-2-((9-Phenanthrenylmethyl)amino)-2-methyl-1,3-butanediol hydrochlorideHCID 86741971—
생성물3-Methoxy-2-methyl-2-((9-phenanthrenylmethyl)amino)-1-propanol hydrochlorideHCID 21273677—

반응 단계

Using the reductive amination procedure outlined in 7G, phenanthrene-9-carbaldehyde (Aldrich) and 2-amino-3-methoxy-2-methyl-1-propanol (9C) gave 3-methoxy-2-methyl-2-((9-phenanthrenylmethyl)amino)-1-propanol hydrochloride mp 211°-213° (dec), (EtOH/Et2O), (C, H, Cl, N).

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US04808625
출처 데이터셋uspto-grants-1989_02
ORD IDord-ea5d76f3f7d4440ba7b723b82f674e32
출처 메모uspto-grants-1989_02