참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Fumaronitrile | HCID 637930 | — |
| 반응물 | [2,6-Dichloro-4-(trifluoromethyl)phenyl]hydrazine | HCID 688223 | — |
| 용매 | Dimethyl Sulfoxide | HCID 679 | — |
| 용매 | Water | HCID 962 | — |
| 생성물 | 2-(2,6-Dichloro-4-trifluoromethylphenylhydrazino)succinonitrile | HCID 53933941 | — |
반응 단계
A mixture of 2,6-dichloro-4-trifluoromethylphenylhydrazine (1.0 g) and fumaronitrile (1.0 g) in dimethylsulfoxide (10 ml) was heated at 100° C. for 7 hours. The cooled mixture was diluted with water and extracted (ether) to give, after evaporation and crystallization from dichloromethane/hexane, the title compound (0.828 g, 63%), m.p. 101-102° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US06258973B1 |
|---|
| 출처 데이터셋 | uspto-grants-2001_07 |
|---|
| ORD ID | ord-354d5861b8424fd79a9ed8aba10df099 |
|---|
| 출처 메모 | uspto-grants-2001_07 |
|---|
