3-Chloroaniline → HCID 54366796, 화합물
반응식
[CH:1]1([N:6]2[C:14]3[C:9](=[CH:10][CH:11]=[C:12]([C:15]([OH:17])=O)[CH:13]=3)[C:8]([CH2:18][CH3:19])=[N:7]2)[CH2:5][CH2:4][CH2:3][CH2:2]1.[Cl:20][C:21]1[CH:22]=[C:23]([CH:25]=[CH:26][CH:27]=1)[NH2:24]>>[Cl:20][C:21]1[CH:22]=[C:23]([NH:24][C:15]([C:12]2[CH:13]=[C:14]3[C:9]([C:8]([CH2:18][CH3:19])=[N:7][N:6]3[CH:1]3[CH2:2][CH2:3][CH2:4][CH2:5]3)=[CH:10][CH:11]=2)=[O:17])[CH:25]=[CH:26][CH:27]=1참가 물질
3
실험 절차
This compound was prepared according to the method of Example 11, using 150 mg (0.581 mmol, 1.0 equiv) 1-cyclopentyl-3-ethyl-1H-indazole-6-carboxylic acid and 68 μL (0.639 mmol, 1.1 equiv) 3-chloro-aniline as starting materials to give 211 mg (99%) of a clear oil; HRMS calcd for C21H22N3OCl+H: 368.1532. Found: 368.1567.
후처리
- customThis compound was prepared
출처 및 근거
- ORD 기록
- ord-7f83a1eea116499cb077908f9f16d529
- 출처 데이터셋
- uspto-grants-2001_07