Dimedone → HCID 9927530, 화합물

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[CH3:1][C:2]1([CH3:15])[CH2:13][C:12](=[O:14])[C:5]2[C:6]([C:9]([OH:11])=O)=[CH:7][O:8][C:4]=2[CH2:3]1.CC1(C)CC(=O)CC(=O)C1.[F:26][C:27]1[CH:33]=[C:32]([O:34][CH3:35])[CH:31]=[CH:30][C:28]=1[NH2:29]>>[F:26][C:27]1[CH:33]=[C:32]([O:34][CH3:35])[CH:31]=[CH:30][C:28]=1[NH:29][C:9]([C:6]1[C:5]2[C:12](=[O:14])[CH2:13][C:2]([CH3:1])([CH3:15])[CH2:3][C:4]=2[O:8][CH:7]=1)=[O:11]

참가 물질

반응물 3

HCID 31358Dimedone

HCID 7971096,6-Dimethyl-4-oxo-4,5,6,7-tetrahydro-benzofuran-3-carboxylic acid

HCID 37563832-Fluoro-4-methoxyaniline

생성물 1

HCID 9927530HCID 9927530, 화합물

실험 절차

Starting with (6,6-dimethyl-4-oxo4,5,6,7-tetrahydro-benzofuran-3-carboxylic acid), prepared from dimedone by Procedure A, and 2-fluoro-4-methoxyaniline, General Procedure B provided the title compound as a white solid:

출처 및 근거

ORD 기록: ord-a990e1af7ac54927a7051da8fffbebf2
출처 데이터셋: uspto-grants-2001_07
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US06262272B1

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