Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Thionyl Chloride → 2-(4-ethoxyphenyl)acetyl Chloride
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Thionyl Chloride | HCID 24386 | — |
| 반응물 | Benzeneacetic acid, 4-ethoxy- | HCID 78631 | — |
| 생성물 | 2-(4-ethoxyphenyl)acetyl Chloride | HCID 11629782 | — |
반응 단계
50 g (0.28 mol) of 4-ethoxyphenylacetic acid were treated with 50 ml of thionyl chloride and the mixture was stirred for 24 hours at room temperature. Excess thionyl chloride was removed in vacuo and the residue was distilled under a high vacuum. This gave 39 g (71% of theory) of an oil (boiling point 110° C./53.3 Pa).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06265398B1 |
| 출처 데이터셋 | uspto-grants-2001_07 |
| ORD ID | ord-ab873478ff5c4224a1fffcfd1c5328c0 |
| 출처 메모 | uspto-grants-2001_07 |