Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Tetrafluoroboric acid → Tricyclohexylphosphonium tetraphenylborate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Tetrafluoroboric acid | HCID 28118 | — |
| 반응물 | Tricyclohexylphosphine | HCID 75806 | — |
| 반응물 | Sodium Tetraphenylborate | HCID 2723787 | — |
| 반응물 | Tricyclohexylphosphonium Tetrafluoroborate | HCID 11710396 | — |
| 생성물 | Tricyclohexylphosphonium tetraphenylborate | HCID 23136635 | 75% |
반응 단계
Tricyclohexylphosphine is reacted with fluoroboric acid to synthesize tricyclohexylphosphonium tetrafluoroborate, which is reacted with sodium tetraphenylborate to produce tricyclohexylphosphonium tetraphenylborate (75% yield). A similar process is described in which tri-tert-butylphosphine is used as starting material to produce tri-tert-butylphosphonium tetraphenylborate (71% yield) (see Nonpatent Document 4).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07728176B2 |
| 출처 데이터셋 | uspto-grants-2010_06 |
| ORD ID | ord-26bcb57d0e5a476a8aaa17b3207a4354 |
| 출처 메모 | uspto-grants-2010_06 |