Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
1,1,1,3,3,3-Hexafluoro-2-propanol → Tri-tert-butylphosphonium Tetraphenylborate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 1,1,1,3,3,3-Hexafluoro-2-propanol | HCID 13529 | — |
| 반응물 | Tris(1,1-dimethylethyl)phosphine | HCID 83681 | — |
| 반응물 | Sodium Tetraphenylborate | HCID 2723787 | — |
| 생성물 | Tri-tert-butylphosphonium Tetraphenylborate | HCID 23136663 | 77% |
반응 단계
Tri-tert-butylphosphine is reacted with 1,1,1,3,3,3-hexafluoro-2-propanol and with sodium tetraphenylborate to produce tri-tert-butylphosphonium tetraphenylborate (77% yield). A similar process is described in which tricyclohexylphosphine is used as starting material to produce tricyclohexylphosphonium tetraphenylborate (77% yield) (see Nonpatent Document 7).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07728176B2 |
| 출처 데이터셋 | uspto-grants-2010_06 |
| ORD ID | ord-32062efb59614351b3cd53ae313ef854 |
| 출처 메모 | uspto-grants-2010_06 |