Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
(4-Methoxyphenyl)boronic acid → 2-(4-Methoxyphenyl)-3-(4-methoxyphenoxy)benzo[b]thiophene
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | (4-Methoxyphenyl)boronic acid | HCID 201262 | — |
| 반응물 | 2-Iodo-3-(4-methoxyphenoxy)benzo[b]thiophene | HCID 10691279 | — |
| 용매 | Ethyl Acetate | HCID 8857 | — |
| 생성물 | 2-(4-Methoxyphenyl)-3-(4-methoxyphenoxy)benzo[b]thiophene | HCID 11793004 | 70% |
반응 단계
By essentially following the procedure detailed in Example 1, Part B, the title compound was prepared from 2-iodo-3-(4-methoxyphenoxy)benzo[b]thiophene (Part B) and (4-methoxyphenyl)boronic acid (Part C) in 70% yield following chromatography (SiO2; 5% EtOAc in hexanes).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06265575B1 |
| 출처 데이터셋 | uspto-grants-2001_07 |
| ORD ID | ord-c0ce58324bd54ddb9494a30ba4e3b937 |
| 출처 메모 | uspto-grants-2001_07 |