Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
3,5-Dichlorobenzenesulfonyl chloride → 3-(3,5-Dichloro-benzenesulfonylamino)-4-methoxy-N-(3,4-dichlorophenyl)-benzamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 3,5-Dichlorobenzenesulfonyl chloride | HCID 522388 | — |
| 반응물 | 3-Amino-4-methoxy-N-(3,4-dichlorophenyl)-benzamide | HCID 9948627 | — |
| 촉매 | 4-(Dimethylamino)pyridine | HCID 14284 | — |
| 생성물 | 3-(3,5-Dichloro-benzenesulfonylamino)-4-methoxy-N-(3,4-dichlorophenyl)-benzamide | HCID 18626055 | 98% |
반응 단계
Prepared according to the procedure described for Example 116 using 3-amino-4-methoxy-N-(3,4-dichlorophenyl)-benzamide from Example 4 (0.932 g, 3.00 mmol), 3,5-dichlorobenzenesulfonyl chloride (0.737 g, 3.00 mmol) and 4-dimethylaminopyridine to afford the product (1.53 g); m.p. >230° C. (dec).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06268387B1 |
| 출처 데이터셋 | uspto-grants-2001_07 |
| ORD ID | ord-33143c8100694c8581396f9902000b25 |
| 출처 메모 | uspto-grants-2001_07 |