Acetic Acid → 4-Chloro-3-methylbut-2-en-1-yl acetate

반응식

[Cl:1]OC(C)(C)C.[CH2:7]=[CH:8][C:9](=[CH2:11])[CH3:10].[C:12]([OH:15])(=[O:14])[CH3:13]>>[Cl:1][CH2:11][C:9]([CH3:10])=[CH:8][CH2:7][O:14][C:12](=[O:15])[CH3:13]

참가 물질

반응물 3

HCID 176Acetic Acid

HCID 6557Isoprene

HCID 521297Tert-Butyl hypochlorite

생성물 1

HCID 534009324-Chloro-3-methylbut-2-en-1-yl acetate

실험 절차

1-Chloro-2-methyl-4-acetoxy-2-butene was prepared in accordance with the process described in J. Am. Chem. Soc. 72 4610 (1950) by reacting t-butyl hypochlorite with isoprene in an acetic acid medium.

출처 및 근거

ORD 기록: ord-7cd93b48c251435dba1ab2fb7bbf8504
출처 데이터셋: uspto-grants-1984_02
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US04433171

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