Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Allyl bromide → N,N-Dimethyl-N-(prop-2-en-1-yl)octadecan-1-aminium chloride
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Allyl bromide | HCID 7841 | — |
| 반응물 | Allyl chloride | HCID 7850 | — |
| 반응물 | Dimethyloctadecylamine | HCID 15365 | — |
| 반응물 | Sodium Bicarbonate | HCID 516892 | — |
| 용매 | Isopropanol | HCID 3776 | — |
| 생성물 | N,N-Dimethyl-N-(prop-2-en-1-yl)octadecan-1-aminium chloride | HCID 20468836 | — |
반응 단계
A 2-liter reaction vessel equipped with a mechanical stirrer and a reflux condenser was charged with 660.0 gm. dimethyl octadecyl amine, 199.0 gm. (2.19 mol) allyl chloride, 13.3 (0.11 mol) gm. allyl bromide, 20 gm. sodium bicarbonate, and 350 ml. isopropyl alcohol. This mixture was heated under reflux overnight. Analyses of a filtered aliquot indicated the reaction was complete. The mixture was filtered and upon analysis had an Effective gram MW of 496.74.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04434076 |
| 출처 데이터셋 | uspto-grants-1984_02 |
| ORD ID | ord-31c201d1fc7b4a01b6dd2e904ca8cfbe |
| 출처 메모 | uspto-grants-1984_02 |