참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Ethanol | HCID 702 | — |
| 반응물 | Diisobutyl aluminium chloride | HCID 16686353 | — |
| 용매 | Toluene | HCID 1140 | — |
| 생성물 | Chloro-ethoxy-isobutyl-aluminum | HCID 20469170 | — |
반응 단계
A solution of 23.75 g (0.516 mol) of absolute ethanol in 350 ml of absolute toluene is added dropwise during 1 hour to a solution of 91.1 g (0.516 mol) of diisobutylaluminum chloride in 350 ml of absolute toluene at 0° C. and under a protective gas atmosphere (argon). Thereafter, the mixture is warmed at 50° C. for 1 hour and cooled to 5° C., to yield the chloro-ethoxy-isobutyl-aluminum starting material.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US04434178 |
|---|
| 출처 데이터셋 | uspto-grants-1984_02 |
|---|
| ORD ID | ord-c8ad5093cd0d48f5a3d2cf671473dfae |
|---|
| 출처 메모 | uspto-grants-1984_02 |
|---|
