Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Acetone → HCID 88766983, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Acetone | HCID 180 | — |
| 반응물 | N,N,N',N',N''-Pentamethylguanidine | HCID 139457 | — |
| 반응물 | HCID 178511210 | HCID 178511210 | — |
| 용매 | Triethylamine | HCID 8471 | — |
| 생성물 | HCID 88766983 | HCID 88766983 | 88% |
반응 단계
To a mixture of 0.1 mol of bis(2-cyanoethyl)phosphine oxide and 0.1 mol of acetone was added 1.0 gram of either triethyl amine or pentamethyl guanidine. The mixture was heated for 2 hours at steam bath temperatures. The resulting solid was filtered and recrystallized from acetone to give an 88% yield of product, m.p. 124°-125° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04247447 |
| 출처 데이터셋 | uspto-grants-1981_01 |
| ORD ID | ord-842a394f7c5a4c3cb602647f6bf0e708 |
| 출처 메모 | uspto-grants-1981_01 |